C₃₀H₄₄O₂Si

Base Information

• Chemical Name: C₃₀H₄₄O₂Si
• CAS No.: 1354779-84-2
• Molecular Formula: C₃₀H₄₄O₂Si
• Molecular Weight: 464.764
• Mol file: 1354779-84-2.mol

Synonyms:C₃₀H₄₄O₂Si

Chemical Property of C₃₀H₄₄O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₄O₂Si

There total 6 articles about C₃₀H₄₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C30H44O2Si (1354779-74-0) → C30H44O2Si (1354779-84-2)

Guidance literature:

With dmap; (+)-10-camphorsulfonic acid; dicyclohexyl-carbodiimide; In dichloromethane;

Reference yield:

tert-butyldiphenyl {[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]oxy}silane (151409-23-3) → C30H44O2Si (1354779-84-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane

2: periodic acid / tetrahydrofuran

3: magnesium / methanol

4: dicyclohexyl-carbodiimide; (+)-10-camphorsulfonic acid; dmap / dichloromethane

With dmap; magnesium; (+)-10-camphorsulfonic acid; periodic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

Farnesol (106-28-5) → C30H44O2Si (1354779-84-2)

Guidance literature:

Multi-step reaction with 5 steps

1: 1H-imidazole / dichloromethane; N,N-dimethyl-formamide

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane

3: periodic acid / tetrahydrofuran

4: magnesium / methanol

5: dicyclohexyl-carbodiimide; (+)-10-camphorsulfonic acid; dmap / dichloromethane

With 1H-imidazole; dmap; magnesium; (+)-10-camphorsulfonic acid; periodic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

Farnesol

tert-butylchlorodiphenylsilane

tert-butyldiphenyl {[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]oxy}silane

tert-butyl(((2E,6E)-9-(3,3-dimethyloxiran-2-yl)-3,7-dimethylnona-2,6-dien-1-yl)oxy)diphenylsilane

Refernces