(1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine

Base Information

Chemical Name:(1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine
CAS No.:181633-59-0
Molecular Formula:C₂₈H₃₇NO₂Si
Molecular Weight:447.693
Hs Code.:

Synonyms:(1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine

Chemical Property:

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Technology Process of (1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine

There total 4 articles about (1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 181633-65-8
[(1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propyl]-carbamic acid tert-butyl ester

: 181633-59-0
(1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; Ambient temperature;
DOI:10.1021/jo960532r

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 181633-59-0
(1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent

2: 94 percent / TFA / CH₂Cl₂ / Ambient temperature

With trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo960532r

Reference yield:

: 181633-58-9
((1R,2R)-1-Benzyloxymethyl-3-hydroxy-2-methyl-propyl)-carbamic acid tert-butyl ester

: 181633-59-0
(1R,2R)-1-Benzyloxymethyl-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent

2: 94 percent / TFA / CH₂Cl₂ / Ambient temperature

With trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo960532r