Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄

Base Information

Chemical Name:Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄
CAS No.:206761-46-8
Molecular Formula:BF₄*C₂₀H₁₅NO₆Re
Molecular Weight:638.354
Hs Code.:

Re(CO)4(OC(OCH<sub>3</sub>)CH<sub>2</sub>NC(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=[Re(CO)4(OC(OCH<sub>3</sub>)CH<sub>2</sub>NC(C<sub>6</sub>H<sub>5</sub>)2)]BF<sub>4</sub>

Synonyms:Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄

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Chemical Property of Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄

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Technology Process of Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄

There total 2 articles about Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: tetrafluoroboric acid

: 206761-36-6
Re(CO)4(C₆H₄C(C₆H₅)NCH₂COOCH₃)

: 206761-46-8
Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄

Guidance literature:: In diethyl ether; dichloromethane; N2-atmosphere; dropwise addn. of HBF4 (in ether) to Re-complex soln. (inCH2Cl2) at 0°C, stirring (room temp., 2 h); concn., pptn. on pentane addn., washing (pentane), drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(97)00579-2

Reference yield:

: 81167-39-7
methyl N-(diphenylmethylene)glycinate

: 206761-46-8
Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄

Guidance literature:: Multi-step reaction with 2 steps

1: octane

2: dichloromethane; diethyl ether

In octane; diethyl ether; dichloromethane;
DOI:10.1016/S0022-328X(97)00579-2

Reference yield: 65.0%

: 78670-77-6
{(pentacarbonyl)rhenium(ethylene)}BF₄

: 206761-46-8
Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH₂NC(C₆H₅)2)]BF₄

: 253304-78-8
Re(CO)4(OC(OCH₃)CH(NC(C₆H₅)2))CH₂CH₂Re(CO)5⁽¹⁺⁾*BF₄^(1-)=[Re(CO)4(OC(OCH₃)CH(NC(C₆H₅)2))CH₂CH₂Re(CO)5]BF₄

Guidance literature:: With sodium hexamethyldisilazane; In dichloromethane; Ar-atmosphere; addn. of NaN(SiMe3)3 (in PhMe) to peptide complex (in CH2Cl2) at -78°C, warming to room temp., concn., pentane addn, centrifugation, evapn., dissoln. in CH2Cl2, addn. of ethylene complex (-78°C), then 1-2 h at room temp.; concn., pptn. on pentane addn., washing (pentane), drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(99)00384-8