4,5-DI-O-ACETYL-2,6-ANHYDRO-3-DEOXY-D-ERYTHRO-HEX-2-ENONONITRILE

Base Information

• Chemical Name: 4,5-DI-O-ACETYL-2,6-ANHYDRO-3-DEOXY-D-ERYTHRO-HEX-2-ENONONITRILE
• CAS No.: 120085-65-6
• Molecular Formula: C₁₀H₁₁NO₅
• Molecular Weight: 225.201
• Mol file: 120085-65-6.mol

Synonyms:4,5-DI-O-ACETYL-2,6-ANHYDRO-3-DEOXY-D-ERYTHRO-HEX-2-ENONONITRILE

Chemical Property of 4,5-DI-O-ACETYL-2,6-ANHYDRO-3-DEOXY-D-ERYTHRO-HEX-2-ENONONITRILE

Chemical Property:

• Boiling Point: 329.9±42.0 °C(Predicted)
• PSA: 85.62000
• Density: 1.27±0.1 g/cm3(Predicted)
• LogP: 0.28748

Purity/Quality:

95% ^*data from raw suppliers

4,5-Di-O-acetyl-2,6-anhydro-3-deoxy-D-erythro-hex-2-enononitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,5-DI-O-ACETYL-2,6-ANHYDRO-3-DEOXY-D-ERYTHRO-HEX-2-ENONONITRILE

There total 2 articles about 4,5-DI-O-ACETYL-2,6-ANHYDRO-3-DEOXY-D-ERYTHRO-HEX-2-ENONONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,3,4-tri-O-acetyl-1-deoxy-1-bromo-α-D-arabinopyranosyl cyanide (89158-09-8) → 4,5-Di-O-acetyl-2,6-anhydro-3-deoxy-D-erythro-hex-2-enononitrile (120085-65-6)

Guidance literature:

With pyridine; zinc; In benzene; for 0.0833333h; Heating;

DOI:10.1016/0008-6215(89)85101-8

Reference yield:

2,3,4-tri-O-acetyl-1-deoxy-1-bromo-α-D-arabinopyranosyl cyanide (89158-09-8) → 4,5-Di-O-acetyl-2,6-anhydro-3-deoxy-D-erythro-hex-2-enononitrile (120085-65-6) + Acetic acid (2S,3R,4R,5R)-3,5-diacetoxy-2-cyano-tetrahydro-pyran-4-yl ester (89158-08-7) + 2,3,4-tri-O-acetyl-α-D-arabinopyranosyl cyanide (82266-99-7)

Guidance literature:

With acetic acid; Product distribution; Ambient temperature; other solvent: benzene, AcOH/water; other temperature: reflux; other additive: pyridine, triethylamine;

upstream raw materials:

2,3,4-tri-O-acetyl-1-deoxy-1-bromo-α-D-arabinopyranosyl cyanide

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