N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin

Base Information

Chemical Name:N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin
CAS No.:126133-72-0
Molecular Formula:C₄₅H₅₄N₄O₂₀
Molecular Weight:970.939
Hs Code.:

Synonyms:N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin

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Chemical Property of N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin

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Technology Process of N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin

There total 4 articles about N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 126133-64-0
N-Allyloxycarbonyl-L-serin-tert-butylester

: 87376-57-6
2-azido-4,6-di-O-benzoyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyl bromide

: N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-β-D-galactopyranosyl)>-L-serin

: 126133-72-0
N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin

Guidance literature:: With 4 A molecular sieve; silver perchlorate; In dichloromethane; toluene; at -50 ℃; for 30h;

Reference yield:

: 90508-22-8
(S)-2-(((allyloxy)carbonyl)amino)-3-hydroxypropanoic acid

: 126133-72-0
N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: konz. H₂SO₄ / CH₂Cl₂ / 24 h / Ambient temperature

3: N₂H₄*H₂O / ethanol / 1 h

4: 76 percent / molecular sieve (4 Angstroem), AgClO₄ / CH₂Cl₂; toluene / 30 h / -50 °C

With 4 A molecular sieve; sulfuric acid; silver perchlorate; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; toluene;

Reference yield:

: 126133-60-6
O-Acetoacetyl-N-allyloxycarbonyl-L-serin

: 126133-72-0
N-Allyloxycarbonyl-O-<(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-O-(2-azido-4,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)>-L-serin

Guidance literature:: Multi-step reaction with 3 steps

1: konz. H₂SO₄ / CH₂Cl₂ / 24 h / Ambient temperature

2: N₂H₄*H₂O / ethanol / 1 h

3: 76 percent / molecular sieve (4 Angstroem), AgClO₄ / CH₂Cl₂; toluene / 30 h / -50 °C

With 4 A molecular sieve; sulfuric acid; silver perchlorate; hydrazine hydrate; In ethanol; dichloromethane; toluene;