N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide

Base Information

Chemical Name:N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide
CAS No.:1092938-44-7
Molecular Formula:C₂₁H₂₆N₄O
Molecular Weight:350.464
Hs Code.:

Synonyms:N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide

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Chemical Property of N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide

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Technology Process of N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide

There total 4 articles about N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1092938-46-9
N₄-(2,6-dimethylbenzyl)-N₆,1,2-trimethyl-1H-benzimidazole-4,6-diamine

: 108-24-7
acetic anhydride

: 1092938-44-7
N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 713529-91-0
4-(2,6-dimethyl-benzylamino)-1,2-dimethyl-1H-benzimidazole-6-carboxylic acid

: 1092938-44-7
N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / 1.5 h / Heating / reflux

2.1: hydrogenchloride / methanol / 45 °C

3.1: sodium methylate / methanol / 1 h / Heating / reflux

3.2: 1 h / Heating / reflux

4.1: dmap / dichloromethane / 2 h / 20 °C

With hydrogenchloride; dmap; diphenyl phosphoryl azide; sodium methylate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;

Reference yield:

: 1092938-88-9
N₄-(2,6-dimethylbenzyl)-1,2-trimethyl-1H-benzimidazole-4,6-diamine

: 1092938-44-7
N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 1 h / Heating / reflux

1.2: 1 h / Heating / reflux

2.1: dmap / dichloromethane / 2 h / 20 °C

With dmap; sodium methylate; In methanol; dichloromethane;