1h,1h-Perfluoro-3,6-dioxadecan-1-ol

Base Information

• Chemical Name: 1h,1h-Perfluoro-3,6-dioxadecan-1-ol
• CAS No.: 152914-73-3
• Molecular Formula: C8H3 F15 O3
• Molecular Weight: 190.14
• Hs Code.: 2909499000
• European Community (EC) Number: 671-182-2
• DSSTox Substance ID: DTXSID50381038
• Wikidata: Q82171614
• Mol file: 152914-73-3.mol

Synonyms:1h,1h-perfluoro-3,6-dioxadecan-1-ol;152914-73-3;2,2-difluoro-2-[1,1,2,2-tetrafluoro-2-(1,1,2,2,3,3,4,4,4-nonafluorobutoxy)ethoxy]ethanol;fluorinated diethylene glycol monobutyl ether;2,2-difluoro-2-(1,1,2,2-tetrafluoro-2-(perfluorobutoxy)ethoxy)ethanol;2,2-Difluoro-2-[1,1,2,2-Tetrafluoro-2-(1,1,2,2,3,3,4,4,4-Nonafluorobutoxy)Ethoxy]-Ethanol;SCHEMBL869241;DTXSID50381038;ZPLAXWXACBJHSW-UHFFFAOYSA-N;MFCD03094403;AKOS015910950;Fluorinated diethyleneglycol monobutyl ether;FT-0676879;A809357;Ethanol,2,2-difluoro-2-[1,1,2,2-tetrafluoro-2-(1,1,2,2,3,3,4,4,4-nonafluorobutoxy)ethoxy]-

Chemical Property of 1h,1h-Perfluoro-3,6-dioxadecan-1-ol

Chemical Property:

• Vapor Pressure: 0.0398mmHg at 25°C
• Boiling Point: 212°Cat760mmHg
• PKA: 13.13±0.10(Predicted)
• Flash Point: 105.9°C
• PSA: 38.69000
• Density: 1.708g/cm³
• LogP: 4.21600
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 18
• Rotatable Bond Count: 8
• Exact Mass: 431.9842664
• Heavy Atom Count: 26
• Complexity: 496

Purity/Quality:

98%min ^*data from raw suppliers

1H,1H-Perfluoro-3,6-dioxadecan-1-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(OC(C(OC(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)O

Technology Process of 1h,1h-Perfluoro-3,6-dioxadecan-1-ol

There total 1 articles about 1h,1h-Perfluoro-3,6-dioxadecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl perfluoro-2-(butoxyethoxy)acetate (129301-40-2) → 2-[2-(nonafluorobutoxy)-tetrafluoroethoxy]-2,2-difluoro-1-ethanol (152914-73-3)

Guidance literature:

With sodium borohydrid; sulfuric acid; In methanol; water;

Reference yield:

3-(2-[2-(nonafluorobutoxy)tetrafluoroethoxy]-2,2-difluoroethoxy)-(R)-2-fluoropropyl-1-p-toluenesulfonate + 2-[2-(nonafluorobutoxy)-tetrafluoroethoxy]-2,2-difluoro-1-ethanol (152914-73-3) + 2-(4-hydroxyphenyl)-5-n-hexylpyrimidine (58415-61-5) → 5-hexyl-2-[4-((R)-2-fluoro-3-(2-(2-(nonafluorobutoxy)tetrafluoroethoxy)-2,2,-difluoroethoxy)propoxy)phenyl]pyrimidine (184350-44-5)

Guidance literature:

With potassium carbonate; In acetonitrile;

Reference yield:

2-[2-(nonafluorobutoxy)-tetrafluoroethoxy]-2,2-difluoro-1-ethanol (152914-73-3) + (S)-5-octyloxy-2-[4-(2,3-oxiranylpropoxy)phenyl]pyrimidine + octanol (111-87-5) → 5-n-octyloxy-2-(4-hydroxyphenyl)-pyrimidine (104539-91-5)

Guidance literature:

upstream raw materials:

methyl perfluoro-2-(butoxyethoxy)acetate

Downstream raw materials:

5-hexyl-2-[4-((R)-2-fluoro-3-(2-(2-(nonafluorobutoxy)tetrafluoroethoxy)-2,2,-difluoroethoxy)propoxy)phenyl]pyrimidine

5-n-octyloxy-2-(4-hydroxyphenyl)-pyrimidine

Refernces

• 1、 -. "Liquid crystal compounds having perfluoroether terminal portions". . . Retrieved 2008/06/13.