4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane

Base Information

Chemical Name:4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane
CAS No.:1320246-23-8
Molecular Formula:C₂₉H₃₂N₂O₁₀
Molecular Weight:568.58
Hs Code.:

Synonyms:4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane

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Chemical Property of 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane

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Technology Process of 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane

There total 2 articles about 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 1320246-23-8
4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen bromide / dichloromethane; acetic acid / 7 h / 0 °C

2: tetrabutyl ammonium fluoride; sodium hydroxide / dichloromethane; water / 48 h / 20 °C

3: trifluoroacetic acid / 2 h / 20 °C

With tetrabutyl ammonium fluoride; hydrogen bromide; trifluoroacetic acid; sodium hydroxide; In dichloromethane; water; acetic acid;
DOI:10.1142/S1088424611003252

Reference yield:

: 6919-96-6
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1320246-23-8
4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride; sodium hydroxide / dichloromethane; water / 48 h / 20 °C

2: trifluoroacetic acid / 2 h / 20 °C

With tetrabutyl ammonium fluoride; trifluoroacetic acid; sodium hydroxide; In dichloromethane; water;
DOI:10.1142/S1088424611003252

Reference yield: 51.2%

: 2975-46-4
3-(trimethylsilyl)prop-2-yn-1-al

: 1320246-23-8
4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane

: 5,15-bis[(trimethylsilyl)ethynyl]-10,20-bis[4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl]porphyrin

Guidance literature:: 3-(trimethylsilyl)prop-2-yn-1-al; 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)phenyl-2,2'-dipyrromethane; With trifluoroacetic acid; In dichloromethane; for 0.5h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1142/S1088424611003252