13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine

Base Information

Chemical Name:13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine
CAS No.:76945-00-1
Molecular Formula:C₂₆H₂₀N₂O
Molecular Weight:376.458
Hs Code.:

13-benzyl-5-oxo-5,7,8,13-tetrahydrobenz<g>indolo<2,3-a>quinolizine

Synonyms:13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine

Chemical Property:

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Technology Process of 13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine

There total 7 articles about 13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 76944-97-3
9-Benzyl-2-(2-chloromethyl-benzoyl)-2,3,4,9-tetrahydro-1H-β-carboline-1-carbonitrile

: 76945-00-1
13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: C₂₇H₂₄N₂O₂

: 76945-00-1
13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine

Guidance literature:: With caesium carbonate; In methanol; at 25 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.201607832

Reference yield:

: 42908-86-1
2-Chloromethylbenzoyl chloride

: 76945-00-1
13-benzyl-5-oxo-5,7,8,13-tetrahydrobenzindolo<2,3-a>quinolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / CH₂Cl₂

2: 92 percent / NaH / dimethylformamide / Ambient temperature

With sodium hydride; In dichloromethane; N,N-dimethyl-formamide;