cyclohex-2-en-1-yl (1a,2,3,7b-tetrahydronaphtho[1,2-b]oxiren-7b-yl) carbonate

Base Information

Chemical Name:cyclohex-2-en-1-yl (1a,2,3,7b-tetrahydronaphtho[1,2-b]oxiren-7b-yl) carbonate
CAS No.:1401427-35-7
Molecular Formula:C₁₇H₁₈O₄
Molecular Weight:286.328
Hs Code.:

Synonyms:cyclohex-2-en-1-yl (1a,2,3,7b-tetrahydronaphtho[1,2-b]oxiren-7b-yl) carbonate

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Chemical Property of cyclohex-2-en-1-yl (1a,2,3,7b-tetrahydronaphtho[1,2-b]oxiren-7b-yl) carbonate

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Technology Process of cyclohex-2-en-1-yl (1a,2,3,7b-tetrahydronaphtho[1,2-b]oxiren-7b-yl) carbonate

There total 2 articles about cyclohex-2-en-1-yl (1a,2,3,7b-tetrahydronaphtho[1,2-b]oxiren-7b-yl) carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: cyclohex-2-en-1-yl 3,4-dihydronaphthalen-1-yl carbonate

: 1401427-35-7
cyclohex-2-en-1-yl (1a,2,3,7b-tetrahydronaphtho[1,2-b]oxiren-7b-yl) carbonate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1002/anie.201203663

Reference yield:

: 141037-04-9
cyclohex-2-en-1-yl 1H-imidazole-1-carboxylate

: 1401427-35-7
cyclohex-2-en-1-yl (1a,2,3,7b-tetrahydronaphtho[1,2-b]oxiren-7b-yl) carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hexamethyldisilazane / 1,2-dimethoxyethane / 1 h / -78 °C / Inert atmosphere

1.2: 2.17 h / -78 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 20 °C

With sodium hexamethyldisilazane; 3-chloro-benzenecarboperoxoic acid; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1002/anie.201203663