6-anilino-1,3λ⁴δ²,5,2,4-trithiadiazepine

Base Information

• Chemical Name: 6-anilino-1,3λ⁴δ²,5,2,4-trithiadiazepine
• CAS No.: 131980-73-9
• Molecular Formula: C₈H₇N₃S₃
• Molecular Weight: 241.362
• Mol file: 131980-73-9.mol

Synonyms:6-anilino-1,3λ⁴δ²,5,2,4-trithiadiazepine

Chemical Property of 6-anilino-1,3λ⁴δ²,5,2,4-trithiadiazepine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-anilino-1,3λ⁴δ²,5,2,4-trithiadiazepine

There total 2 articles about 6-anilino-1,3λ⁴δ²,5,2,4-trithiadiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

6-bromo-1,3λ4δ2,5,2,4-trithiadiazepine (97484-11-2) + aniline (62-53-3) → 6-anilino-1,3λ4δ2,5,2,4-trithiadiazepine (131980-73-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 48h; Ambient temperature;

Reference yield: 70.0%

lithium anilide (20732-26-7,82959-02-2) + 6-bromo-1,3λ4δ2,5,2,4-trithiadiazepine (97484-11-2) → 6-anilino-1,3λ4δ2,5,2,4-trithiadiazepine (131980-73-9)

Guidance literature:

In tetrahydrofuran; Ambient temperature;

DOI:10.1039/c39900001315

upstream raw materials:

lithium anilide

6-bromo-1,3λ⁴δ²,5,2,4-trithiadiazepine

aniline