cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one

Base Information

Chemical Name:cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one
CAS No.:126158-30-3
Molecular Formula:C₂₀H₂₀N₂O₄
Molecular Weight:352.39
Hs Code.:

Synonyms:cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one

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Chemical Property of cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one

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Technology Process of cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one

There total 4 articles about cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 126158-20-1
4-(α-methylstyryl)-1-(4-methoxyphenyl)-3-(nitromethylene)azetidin-2-one

: 126158-30-3
cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one

Guidance literature:: With tri-n-butyl-tin hydride; In methanol; dichloromethane; for 24h; Ambient temperature;
DOI:10.1021/jo00294a020

Reference yield:

: 94612-37-0
1-(4-methoxyphenyl)-4-(3-phenylprop-2-en-2-yl)-2,3-azetidinedione

: 126158-30-3
cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

2: 76 percent / tributyltin hydride / CH₂Cl₂; methanol / 24 h / Ambient temperature

With tri-n-butyl-tin hydride; In methanol; dichloromethane;
DOI:10.1021/jo00294a020

Reference yield:

: 121766-42-5,131614-11-4
3-Hydroxy-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-azetidin-2-one

: 126158-30-3
cis-1-(4-methoxyphenyl)-4-(α-methylstyryl)-3-(nitromethyl)azetidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 1) dimethylsulfide, bromine, 2) triethylamine / 1) methylene chloride, 5 min, room temp., 2) methylene chloride, 0 deg C, 1.5h

3: 76 percent / tributyltin hydride / CH₂Cl₂; methanol / 24 h / Ambient temperature

With dimethylsulfide; bromine; tri-n-butyl-tin hydride; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jo00294a020