Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate

Base Information

Chemical Name:Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate
CAS No.:82214-72-0
Molecular Formula:C₂₂H₂₆O₄
Molecular Weight:354.446
Hs Code.:

Synonyms:Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate

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Chemical Property of Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate

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Technology Process of Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate

There total 6 articles about Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82214-71-9
Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohex-2-enecarboxylate

: 82214-72-0
Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;

Reference yield:

: 88-14-2
2-furanoic acid

: 82214-72-0
Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 19 g / AlCl₃

2: 20.4 g / LAH / tetrahydrofuran / 4h, r.t.

3: 21.45 g / PBr₃ / benzene / 1) 0 degC, 45 min 2) 60 degC, 2.5h

4: 1) K-tert-butoxide / 1) benzene 2a) 10h, r.t. 2b) 12h, reflux

5: 1.75 g / H₂ / 10percent Pd-C / aq. ethanol / 760 Torr / Ambient temperature

With lithium aluminium tetrahydride; potassium tert-butylate; hydrogen; phosphorus tribromide; palladium on activated charcoal; aluminium trichloride; In tetrahydrofuran; ethanol; benzene;

Reference yield:

: 61109-49-7
1-Hydroxymethyl-6-methoxynaphthalene

: 82214-72-0
Ethyl 3-(6-methoxy-1-naphthylmethyl)-2-methyl-4-oxo-cyclohexane carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 21.45 g / PBr₃ / benzene / 1) 0 degC, 45 min 2) 60 degC, 2.5h

2: 1) K-tert-butoxide / 1) benzene 2a) 10h, r.t. 2b) 12h, reflux

3: 1.75 g / H₂ / 10percent Pd-C / aq. ethanol / 760 Torr / Ambient temperature

With potassium tert-butylate; hydrogen; phosphorus tribromide; palladium on activated charcoal; In ethanol; benzene;