N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide

Base Information

Chemical Name:N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide
CAS No.:1374209-97-8
Molecular Formula:C₂₆H₂₁BrN₂O₄S
Molecular Weight:537.434
Hs Code.:

Synonyms:N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide

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Chemical Property of N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide

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Technology Process of N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide

There total 5 articles about N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 98-58-8
4-bromobenzenesulfonyl chloride

: 6-(4-amino-butyl)-6H-indeno[1,2-c]isoquinoline-5,11-dione; hydrochloride

: 1374209-97-8
N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide

Guidance literature:: With triethylamine; In chloroform; at 70 ℃; for 16h;
DOI:10.1021/jm300335n

Reference yield: 84.0%

: 1374209-97-8
N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide

Guidance literature:: With triethylamine; In chloroform; for 16h; Reflux;

Reference yield:

: 119-67-5
o-carboxybenzaldehyde

: 1374209-97-8
N-(4-(5,11-dioxo-5H-indeno[1,2-c]isoquinolin-6(11H)-yl)butyl)-4-bromobenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium methylate / methanol; ethyl acetate / 16 h / 70 °C

2: water; toluene-4-sulfonic acid / benzene / 7 h / Reflux

3: chloroform / Reflux

4: hydrogenchloride / methanol / 20 °C

5: triethylamine / chloroform / 16 h / 70 °C

With hydrogenchloride; water; sodium methylate; toluene-4-sulfonic acid; triethylamine; In methanol; chloroform; ethyl acetate; benzene;
DOI:10.1021/jm300335n