tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane

Base Information

• Chemical Name: tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane
• CAS No.: 165288-20-0
• Molecular Formula: C₅₄H₇₈N₄O₈S₄
• Molecular Weight: 1039.5

Synonyms:tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane

Chemical Property of tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane

Chemical Property:

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Technology Process of tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane

There total 3 articles about tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N,N'-bis(2,4,6-trimethylbenzenesulfonyl)-1,4-butanediamine (161452-28-4) + N,O-bis(2,4,6-trimethylbenzenesulfonyl)-4-piperidineethanol (165288-19-7) → tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane (165288-20-0)

Guidance literature:

N,N'-bis(2,4,6-trimethylbenzenesulfonyl)-1,4-butanediamine; With sodium hydride; sodium iodide; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 0.383333h;

N,O-bis(2,4,6-trimethylbenzenesulfonyl)-4-piperidineethanol; In DMF (N,N-dimethyl-formamide); at 20 - 67 ℃; for 18h;

Reference yield:

4-(2-Hydroxyethyl)piperidine (622-26-4) → tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane (165288-20-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / pyridine / 44 h / 5.5 °C

2: 1.) NaH, NaI / 1.) DMF, RT, 23 min, 2.) DMF, from 58 to 67 deg C, 18 h

With pyridine; sodium hydride; sodium iodide;

DOI:10.1021/jm00013a003

Reference yield:

2-mesitylenesulphonyl chloride (773-64-8) → tetrakis(mesitylsulfonyl)-N,N'-bis<2-(4-piperidinyl)ethyl>-1,4-diaminobutane (165288-20-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / pyridine / 44 h / 5.5 °C

2: 1.) NaH, NaI / 1.) DMF, RT, 23 min, 2.) DMF, from 58 to 67 deg C, 18 h

With pyridine; sodium hydride; sodium iodide;

DOI:10.1021/jm00013a003

upstream raw materials:

N,N'-bis(2,4,6-trimethylbenzenesulfonyl)-1,4-butanediamine

N,O-bis(2,4,6-trimethylbenzenesulfonyl)-4-piperidineethanol

4-(2-Hydroxyethyl)piperidine

2-mesitylenesulphonyl chloride

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