1-BOC-6-CHLOROINDOLE

Base Information

Chemical Name:1-BOC-6-CHLOROINDOLE
CAS No.:323580-68-3
Molecular Formula:C13H14ClNO2
Molecular Weight:251.713
Hs Code.:2933990090
Mol file:323580-68-3.mol

Synonyms:6-Chloroindole-1-carboxylicacid tert-butyl ester;tert-Butyl 6-chloroindole-1-carboxylate;

Suppliers and Price of 1-BOC-6-CHLOROINDOLE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
6-Chloroindole,N-BocProtected
100mg
$ 75.00

Crysdot
tert-Butyl6-chloro-1H-indole-1-carboxylate 95+%
25g
$ 313.00

American Custom Chemicals Corporation
1-BOC-6-CHLOROINDOLE 95.00%
5G
$ 1076.73

American Custom Chemicals Corporation
1-BOC-6-CHLOROINDOLE 95.00%
1G
$ 664.82

AK Scientific
1-BOC-6-chloroindole
25g
$ 531.00

AK Scientific
1-BOC-6-chloroindole
5g
$ 211.00

Total 14 raw suppliers

Chemical Property of 1-BOC-6-CHLOROINDOLE

Chemical Property:

Vapor Pressure:4.55E-05mmHg at 25°C
Melting Point:85-87 °C
Refractive Index:1.557
Boiling Point:349.9 °C at 760 mmHg
Flash Point:165.4 °C
PSA：31.23000
Density:1.19 g/cm³
LogP:4.07790
Storage Temp.:Keep Cold

Purity/Quality:

97% ^*data from raw suppliers

6-Chloroindole,N-BocProtected ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-BOC-6-CHLOROINDOLE

There total 3 articles about 1-BOC-6-CHLOROINDOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 323580-68-3
6-chloroindole-1-carboxylic acid tert-butyl ester

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;

Reference yield: 88.0%

: 17422-33-2
6-chloroindole

: 24424-99-5
di-tert-butyl dicarbonate

: 323580-68-3
6-chloroindole-1-carboxylic acid tert-butyl ester

Guidance literature:: With dmap; In tert-butyl methyl ether; at 30 ℃; for 1h;

Reference yield: 84.0%

: 4248-19-5
tert-butyl carbazate

: 1-bromo-2-[2-bromovinyl]-5-chlorobenzene

: 323580-68-3
6-chloroindole-1-carboxylic acid tert-butyl ester

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; In toluene; at 110 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.046