2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate

Base Information

Chemical Name:2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate
CAS No.:1365413-65-5
Molecular Formula:C₁₆H₂₁NO₅
Molecular Weight:307.346
Hs Code.:

Synonyms:2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate

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Chemical Property of 2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate

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Technology Process of 2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate

There total 1 articles about 2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110-89-4
piperidine

: 79236-96-7
2-methoxy-4-(hydroxymethyl)-3-methoxybenzoate

: 530-62-1
1,1'-carbonyldiimidazole

: 1365413-65-5
2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate

Guidance literature:: 2-methoxy-4-(hydroxymethyl)-3-methoxybenzoate; 1,1'-carbonyldiimidazole; In dichloromethane; at 0 - 20 ℃; for 0.833333h;

piperidine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1039/c2cc17566e

Reference yield: 92.0%

: 1365413-65-5
2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate

: 1365413-67-7
3-methoxy-4-{[(piperidin-1-ylcarbonyl)oxy]methyl}benzoic acid

Guidance literature:: 2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate; With lithium hydroxide monohydrate; In tetrahydrofuran; methanol; water; at 20 ℃; for 10h;

With hydrogenchloride; In water;
DOI:10.1039/c2cc17566e

Reference yield:

: 1365413-65-5
2-methoxy-4-(methoxycarbonyl)benzyl piperidine-1-carboxylate

: 1365413-51-9
4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2-methoxybenzyl piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 10 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

3.1: sodium azide / water; acetone / 1 h / 0 °C

4.1: toluene / 1 h / 100 °C

4.2: 10 h / 112 °C

With sodium azide; lithium hydroxide monohydrate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene;
DOI:10.1039/c2cc17566e