phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside

Base Information

Chemical Name:phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside
CAS No.:169962-09-8
Molecular Formula:C₅₃H₄₆O₁₅S
Molecular Weight:955.005
Hs Code.:

Synonyms:phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside

Suppliers and Price of phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside

There total 5 articles about phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: phenyl O-(2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 169962-09-8
phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1002/ejoc.201001690

Reference yield: 87.0%

: 213743-04-5
Phenyl 2,3-di-O-benzoyl-4,6-isopropylidene-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 169962-09-8
phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside

Guidance literature:: With water; trifluoroacetic acid; In tetrahydrofuran; 1.) 0 deg C, 15 min, 2.) r.t., 45 min;
DOI:10.1039/a801429i

Reference yield:

: 27891-73-2,27894-87-7,5329-58-8
β-phenylsulfanyl lactoside

: 169962-09-8
phenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glycopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / acetonitrile / 20 h / 20 °C

2: pyridine / 20 h / 20 °C

3: water; trifluoroacetic acid / dichloromethane / 1 h / 0 °C

With pyridine; water; toluene-4-sulfonic acid; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201001690