2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile

Base Information

Chemical Name:2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile
CAS No.:410082-08-5
Molecular Formula:C₂₇H₂₂N₂O₆
Molecular Weight:470.481
Hs Code.:

Synonyms:2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile

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Chemical Property of 2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile

Chemical Property:

Purity/Quality:

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Technology Process of 2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile

There total 10 articles about 2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 582-25-2
Potassium benzoate

: 410082-08-5
2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile

Guidance literature:: Multi-step reaction with 7 steps

1: 83 percent / dimethylformamide / 48 h / 100 °C

2: 77 percent / NaN₃ / dimethylsulfoxide / 47 h / 115 - 120 °C

3: H₂ / 10 percent Pd/C / ethanol; CHCl₃ / 120 h / 20 °C

4: 4.67 g / pyridine / 96 h / 20 °C

5: CF₃CO₂H; 6M HCl / 96 h / 4 °C

6: NH₂OH*HCl; NaOAc / ethanol; CH₂Cl₂ / 2 h / 20 °C

7: 0.7171 g / MsCl; pyridine / 2.5 h / -15 - 20 °C

With pyridine; hydrogenchloride; sodium azide; hydroxylamine hydrochloride; hydrogen; sodium acetate; methanesulfonyl chloride; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01126-7

Reference yield:

: 157506-35-9
2,5-anhydro-3,6-di-O-methanesulfonyl-D-glucose ethylene acetal

: 410082-08-5
2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile

Guidance literature:: Multi-step reaction with 8 steps

1: 87 percent / Ag₂O / diethyl ether / 22 h / Heating

2: 83 percent / dimethylformamide / 48 h / 100 °C

3: 77 percent / NaN₃ / dimethylsulfoxide / 47 h / 115 - 120 °C

4: H₂ / 10 percent Pd/C / ethanol; CHCl₃ / 120 h / 20 °C

5: 4.67 g / pyridine / 96 h / 20 °C

6: CF₃CO₂H; 6M HCl / 96 h / 4 °C

7: NH₂OH*HCl; NaOAc / ethanol; CH₂Cl₂ / 2 h / 20 °C

8: 0.7171 g / MsCl; pyridine / 2.5 h / -15 - 20 °C

With pyridine; hydrogenchloride; sodium azide; hydroxylamine hydrochloride; hydrogen; sodium acetate; methanesulfonyl chloride; trifluoroacetic acid; silver(l) oxide; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01126-7

Reference yield:

: 228398-97-8
2,5-anhydro-4-O-benzyl-3,6-di-O-methanesulfonyl-D-glucose ethylene acetal

: 410082-08-5
2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allononitrile

Guidance literature:: Multi-step reaction with 7 steps

1: 83 percent / dimethylformamide / 48 h / 100 °C

2: 77 percent / NaN₃ / dimethylsulfoxide / 47 h / 115 - 120 °C

3: H₂ / 10 percent Pd/C / ethanol; CHCl₃ / 120 h / 20 °C

4: 4.67 g / pyridine / 96 h / 20 °C

5: CF₃CO₂H; 6M HCl / 96 h / 4 °C

6: NH₂OH*HCl; NaOAc / ethanol; CH₂Cl₂ / 2 h / 20 °C

7: 0.7171 g / MsCl; pyridine / 2.5 h / -15 - 20 °C

With pyridine; hydrogenchloride; sodium azide; hydroxylamine hydrochloride; hydrogen; sodium acetate; methanesulfonyl chloride; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01126-7