(2-indol-3'-ylethyl)<(3(R)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R)-yl)methyl>amine

Base Information

Chemical Name:(2-indol-3'-ylethyl)<(3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R*)-yl)methyl>amine
CAS No.:101917-40-2
Molecular Formula:C₂₃H₃₆N₂OSi
Molecular Weight:384.637
Hs Code.:

Synonyms:(2-indol-3'-ylethyl)<(3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R*)-yl)methyl>amine

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Chemical Property of (2-indol-3'-ylethyl)<(3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R*)-yl)methyl>amine

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Technology Process of (2-indol-3'-ylethyl)<(3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R*)-yl)methyl>amine

There total 4 articles about (2-indol-3'-ylethyl)<(3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R*)-yl)methyl>amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 101917-35-5
N-(2-indol-3'-ylethyl)-3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-ene-1(R*)-carboxamide

: 101917-40-2
(2-indol-3'-ylethyl)<(3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R*)-yl)methyl>amine

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene; for 3h; Heating;
DOI:10.1021/jo00362a030

Reference yield:

: 4720-83-6
6-oxabicyclo[3.2.1]oct-3-en-7-one

: 101917-40-2
(2-indol-3'-ylethyl)<(3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R*)-yl)methyl>amine

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / chlorobenzene / 20 h / 120 °C

2: 95 percent / imidazole / dimethylformamide / 12 h / Ambient temperature

3: 100 percent / sodium bis(methoxyethoxy)aluminum hydride / tetrahydrofuran; toluene / 3 h / Heating

With 1H-imidazole; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; N,N-dimethyl-formamide; chlorobenzene; toluene;
DOI:10.1021/jo00362a030

Reference yield:

: 61-54-1
tryptamine

: 101917-40-2
(2-indol-3'-ylethyl)<(3(R*)-(tert-butyldimethylsiloxy)cyclohex-4-en-1(R*)-yl)methyl>amine

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / chlorobenzene / 20 h / 120 °C

2: 95 percent / imidazole / dimethylformamide / 12 h / Ambient temperature

3: 100 percent / sodium bis(methoxyethoxy)aluminum hydride / tetrahydrofuran; toluene / 3 h / Heating

With 1H-imidazole; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; N,N-dimethyl-formamide; chlorobenzene; toluene;
DOI:10.1021/jo00362a030