Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester

Base Information

Chemical Name:Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester
CAS No.:209854-85-3
Molecular Formula:C₅₅H₇₆O₉
Molecular Weight:881.203
Hs Code.:

Synonyms:Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester

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Chemical Property of Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester

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Technology Process of Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester

There total 3 articles about Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 209854-84-2
Octadecanoic acid (R)-3-oxo-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester

: 209854-85-3
Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester

Guidance literature:: With zinc(II) tetrahydroborate; In diethyl ether; at 0 ℃;

Reference yield:

: 174501-57-6
Octadecanoic acid (E)-(S)-4-ethoxycarbonyl-2-hydroxy-but-3-enyl ester

: 209854-85-3
Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / AgClO₄, SnCl₂, 4 Angstroem molecular sieves / diethyl ether / -15 °C

2: 1.) O₃, 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C

3: 75 percent / Zn(BH₄)2 / diethyl ether / 0 °C

With zinc(II) tetrahydroborate; 4 A molecular sieve; silver perchlorate; ozone; triphenylphosphine; tin(ll) chloride; In diethyl ether;

Reference yield:

: 209854-83-1
Octadecanoic acid (E)-(S)-4-ethoxycarbonyl-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-but-3-enyl ester

: 209854-85-3
Octadecanoic acid (S)-3-hydroxy-2-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) O₃, 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C

2: 75 percent / Zn(BH₄)2 / diethyl ether / 0 °C

With zinc(II) tetrahydroborate; ozone; triphenylphosphine; In diethyl ether;