4β-(((o-nitrophenyl)selenyl)methyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene

Base Information

Chemical Name:4β-(((o-nitrophenyl)selenyl)methyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene
CAS No.:80595-55-7
Molecular Formula:C₁₉H₂₅NO₂Se
Molecular Weight:378.373
Hs Code.:

Synonyms:4β-(((o-nitrophenyl)selenyl)methyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene

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Chemical Property of 4β-(((o-nitrophenyl)selenyl)methyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene

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Technology Process of 4β-(((o-nitrophenyl)selenyl)methyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene

There total 2 articles about 4β-(((o-nitrophenyl)selenyl)methyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 51694-22-5
ortho-nitrophenyl selenocyanate

: 80656-16-2
4β-(hydroxymethyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene

: 80595-55-7
4β-(((o-nitrophenyl)selenyl)methyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene

Guidance literature:: With tributylphosphine; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1021/ja00372a027

Reference yield:

: 80595-63-7,80657-42-7
5-Isopropyl-2,3,3a,4,5,7a-hexahydro-1H-indene-4-carboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 80595-55-7
4β-(((o-nitrophenyl)selenyl)methyl)-5β-(2-propyl)-2,3,3aβ,4,5,7aα-hexahydroindene

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / LiAlH₄ / diethyl ether

2: 91 percent / n-Bu₃P / tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; tributylphosphine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00372a027