{6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol

Base Information

Chemical Name:{6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol
CAS No.:1187836-49-2
Molecular Formula:C₁₆H₁₆N₆O₂
Molecular Weight:324.342
Hs Code.:

Synonyms:{6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol

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Chemical Property of {6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol

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Technology Process of {6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol

There total 5 articles about {6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1187835-48-8
6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridine-2-carbaldehyde

: 1187836-49-2
{6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol

Guidance literature:: 6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridine-2-carbaldehyde; With sodium tris(acetoxy)borohydride; In tetrahydrofuran; for 20h;

With water; sodium hydroxide; In tetrahydrofuran; for 0.25h;

Reference yield:

: 208111-47-1
(6-[1,3]dioxolan-2-yl-pyridin-2-yl)methanol

: 1187836-49-2
{6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfurous dibromide / dichloromethane / 5 - 20 °C

2.1: DBN / acetonitrile / 0 - 20 °C

3.1: water; toluene-4-sulfonic acid / dimethyl sulfoxide / 1.5 h / 100 °C

4.1: sodium tris(acetoxy)borohydride / tetrahydrofuran / 20 h

4.2: 0.25 h

With sulfurous dibromide; DBN; water; sodium tris(acetoxy)borohydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 897943-12-3
2-[1,3]dioxolan-2-yl-6-methylpyridine 1-oxide

: 1187836-49-2
{6-[({[(1-methyl-1H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}methanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / dichloromethane / 2 h

1.2: 2 h

2.1: sulfurous dibromide / dichloromethane / 5 - 20 °C

3.1: DBN / acetonitrile / 0 - 20 °C

4.1: water; toluene-4-sulfonic acid / dimethyl sulfoxide / 1.5 h / 100 °C

5.1: sodium tris(acetoxy)borohydride / tetrahydrofuran / 20 h

5.2: 0.25 h

With sulfurous dibromide; DBN; water; sodium tris(acetoxy)borohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile;