N¹-(2,4,6-trimethylphenyl)-N²-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Base Information

• Chemical Name: N¹-(2,4,6-trimethylphenyl)-N²-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride
• CAS No.: 1403228-45-4
• Molecular Formula: C₂₁H₂₈N₃*Cl
• Molecular Weight: 357.926

Synonyms:N¹-(2,4,6-trimethylphenyl)-N²-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Chemical Property of N¹-(2,4,6-trimethylphenyl)-N²-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Chemical Property:

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Technology Process of N¹-(2,4,6-trimethylphenyl)-N²-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride

There total 4 articles about N¹-(2,4,6-trimethylphenyl)-N²-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

N1-(2,4,6-trimethylphenyl)-N2-(2-(dimethylamino)benzyl)-1,2-diaminoethane (1403228-44-3) + orthoformic acid triethyl ester (122-51-0) → N1-(2,4,6-trimethylphenyl)-N2-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride (1403228-45-4)

Guidance literature:

With hydrogenchloride; at 100 ℃; for 4h;

DOI:10.1021/om300783g

Reference yield:

2-(dimethylamino)benzaldehyde (579-72-6) → N1-(2,4,6-trimethylphenyl)-N2-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride (1403228-45-4)

Guidance literature:

Multi-step reaction with 3 steps

1: formic acid / methanol / 24 h / 20 °C

2: sodium tetrahydroborate / methanol / 12 h / 20 °C

3: hydrogenchloride / 4 h / 100 °C

With hydrogenchloride; sodium tetrahydroborate; formic acid; In methanol;

DOI:10.1021/om300783g

Reference yield:

C20H27N3 → N1-(2,4,6-trimethylphenyl)-N2-(2-(dimethylamino)benzyl)-4,5-dihydro-1H-imidazol-3-ium chloride (1403228-45-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 12 h / 20 °C

2: hydrogenchloride / 4 h / 100 °C

With hydrogenchloride; sodium tetrahydroborate; In methanol;

DOI:10.1021/om300783g

upstream raw materials:

N¹-(2,4,6-trimethylphenyl)-N²-(2-(dimethylamino)benzyl)-1,2-diaminoethane

orthoformic acid triethyl ester

2-(dimethylamino)benzaldehyde

N-2,4,6-trimethylphenyl-(1,2-diaminoethane)

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