C₄₂H₅₆O₅S₂Si

Base Information

Chemical Name:C₄₂H₅₆O₅S₂Si
CAS No.:1392308-85-8
Molecular Formula:C₄₂H₅₆O₅S₂Si
Molecular Weight:733.121
Hs Code.:

C<sub>42</sub>H<sub>56</sub>O<sub>5</sub>S<sub>2</sub>Si

Synonyms:C₄₂H₅₆O₅S₂Si

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Chemical Property of C₄₂H₅₆O₅S₂Si

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Technology Process of C₄₂H₅₆O₅S₂Si

There total 11 articles about C₄₂H₅₆O₅S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1392308-73-4
C₄₈H₇₀O₅S₂Si₂

: 1392308-85-8
C₄₂H₅₆O₅S₂Si

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 25 ℃; for 9h;
DOI:10.1002/anie.201201653

Reference yield:

: 14947-48-9
2-(2'-hydroxyethyl)-1,3-dithiane

: 1392308-85-8
C₄₂H₅₆O₅S₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: (+)-10-camphorsulfonic acid / dichloromethane / 1 h / 0 °C

2.1: n-butyllithium; dibutylmagnesium / tetrahydrofuran; hexane; n-heptane / 1 h / 25 °C

2.2: 1.5 h / -78 - 0 °C

3.1: zinc(II) chloride / diethyl ether; dichloromethane / 3 h / 25 °C

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

5.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C

5.2: 1 h / -78 - 0 °C

6.1: pyridinium p-toluenesulfonate / ethanol / 9 h / 25 °C

With n-butyllithium; dibutylmagnesium; tert.-butyl lithium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; ethanol; hexane; n-heptane; dichloromethane; pentane; 4.1: Parikh-Doering oxidation;
DOI:10.1002/anie.201201653

Reference yield:

: 1392308-72-3
C₁₈H₃₄O₂S₂Si

: 1392308-85-8
C₄₂H₅₆O₅S₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

2.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C

2.2: 1 h / -78 - 0 °C

3.1: pyridinium p-toluenesulfonate / ethanol / 9 h / 25 °C

With tert.-butyl lithium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In diethyl ether; ethanol; dichloromethane; pentane; 1.1: Parikh-Doering oxidation;
DOI:10.1002/anie.201201653