isobutyl N-phenethylcarbamate

Base Information

Chemical Name:isobutyl N-phenethylcarbamate
CAS No.:208341-61-1
Molecular Formula:C₁₃H₁₉NO₂
Molecular Weight:221.299
Hs Code.:

Synonyms:isobutyl N-phenethylcarbamate

Suppliers and Price of isobutyl N-phenethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isobutyl N-phenethylcarbamate

Chemical Property:

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Technology Process of isobutyl N-phenethylcarbamate

There total 4 articles about isobutyl N-phenethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 64-04-0
phenethylamine

: 543-27-1
isobutyl chloroformate

: 208341-61-1
isobutyl N-phenethylcarbamate

Guidance literature:: With zinc; In benzene; for 0.15h; Ambient temperature;
DOI:10.1016/S0040-4039(98)00464-X

Reference yield:

: C₁₄H₁₉NO₃

: 208341-61-1
isobutyl N-phenethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: tetrabutylammonium perchlorate / 50 °C / Electrochemical reaction; Sealed tube; Inert atmosphere

With tetrabutylammonium perchlorate; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/d0cc05069e

Reference yield:

: 64-04-0
phenethylamine

: 208341-61-1
isobutyl N-phenethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 20 °C

3: tetrabutylammonium perchlorate / 50 °C / Electrochemical reaction; Sealed tube; Inert atmosphere

With tetrabutylammonium perchlorate; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/d0cc05069e