C₄₇H₆₃O₁₃SiN₃

Base Information

Chemical Name:C₄₇H₆₃O₁₃SiN₃
CAS No.:255876-29-0
Molecular Formula:C₄₇H₆₃N₃O₁₃Si
Molecular Weight:906.115
Hs Code.:

C<sub>47</sub>H<sub>63</sub>O<sub>13</sub>SiN<sub>3</sub>

Synonyms:C₄₇H₆₃O₁₃SiN₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₆₃O₁₃SiN₃

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Technology Process of C₄₇H₆₃O₁₃SiN₃

There total 13 articles about C₄₇H₆₃O₁₃SiN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₈H₆₃F₃SO₁₆Si

: 255876-29-0
C₄₇H₆₃O₁₃SiN₃

Guidance literature:: With tetrabutylammoniun azide; In toluene;
DOI:10.1021/ol990245k

Reference yield:

: 255876-13-2
C₁₆H₂₉BrO₆

: 255876-29-0
C₄₇H₆₃O₁₃SiN₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisopropylamine; nBuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C

1.2: 83 percent / HMPA / tetrahydrofuran; hexane / 1 h / -40 °C

2.1: 76 percent / PPTS / ethanol / 10 h / 20 °C

3.1: 4 Angstroem MS; PhSOTf; DTBP / CH₂Cl₂ / 2 h / -78 - -40 °C

4.1: 87 percent / RuCl₃*H₂O; NaIO₄ / ethyl acetate; acetonitrile; H₂O

5.1: pyridine / CH₂Cl₂

6.1: CsOCOCF₃; 18-crown-6 / toluene; dimethylformamide / 80 °C

7.1: 64 percent / imidazole / CH₂Cl₂

8.1: pyridine / CH₂Cl₂

9.1: Bu₄NN₃ / toluene

With pyridine; 1H-imidazole; ruthenium trichloride; sodium periodate; n-butyllithium; 18-crown-6 ether; di-tert-butyl peroxide; 4 Angstroem MS; tetrabutylammoniun azide; pyridinium p-toluenesulfonate; diisopropylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol990245k

Reference yield:

: 255876-14-3
C₅₁H₆₂O₁₃S

: 255876-29-0
C₄₇H₆₃O₁₃SiN₃

Guidance literature:: Multi-step reaction with 8 steps

1: 76 percent / PPTS / ethanol / 10 h / 20 °C

2: 4 Angstroem MS; PhSOTf; DTBP / CH₂Cl₂ / 2 h / -78 - -40 °C

3: 87 percent / RuCl₃*H₂O; NaIO₄ / ethyl acetate; acetonitrile; H₂O

4: pyridine / CH₂Cl₂

5: CsOCOCF₃; 18-crown-6 / toluene; dimethylformamide / 80 °C

6: 64 percent / imidazole / CH₂Cl₂

7: pyridine / CH₂Cl₂

8: Bu₄NN₃ / toluene

With pyridine; 1H-imidazole; ruthenium trichloride; sodium periodate; 18-crown-6 ether; di-tert-butyl peroxide; 4 Angstroem MS; tetrabutylammoniun azide; pyridinium p-toluenesulfonate; In ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol990245k