(3aR*,7R*,7aS*)-N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

Base Information

• Chemical Name: (3aR*,7R*,7aS*)-N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole
• CAS No.: 82281-26-3
• Molecular Formula: C₂₂H₂₁NO₃
• Molecular Weight: 347.414

Synonyms:(3aR*,7R*,7aS*)-N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

Chemical Property of (3aR*,7R*,7aS*)-N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

Chemical Property:

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Technology Process of (3aR*,7R*,7aS*)-N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

There total 12 articles about (3aR*,7R*,7aS*)-N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

(E)-N-benzyl-N-<<3,4-(methylnenedioxy)benzylidene>methyl>-3(E),5-hexadienamide (82293-68-3) → (3aR*,4R*,9aS*)-N-benzyl-2-oxo-4-vinyl-2,3,3a,4,9,9a,-hexahydro-6,7-(methylenedioxy)benzindole (82281-27-4) + N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole (82281-24-1,82281-25-2,82281-26-3)

Guidance literature:

In xylene; for 18h; Heating;

DOI:10.1021/jo00140a008

Reference yield: 27.0%

(E)-N-benzyl-N-<<3,4-(methylenedioxy)benzylidene>methyl>-2-(2,5-dihydro-1,1-dioxothienyl)acetamide (82281-23-0) → N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole (82281-24-1,82281-25-2,82281-26-3) + (3aR*,7R*,7aS*)-N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole (82281-26-3)

Guidance literature:

In xylene; at 150 ℃; for 3.5h; resealable glass bomb;

DOI:10.1021/jo00140a008

Reference yield: 27.0%

(E)-N-benzyl-N-<<3,4-(methylenedioxy)benzylidene>methyl>-2-(2,5-dihydro-1,1-dioxothienyl)acetamide (82281-23-0) → N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole (82281-24-1,82281-25-2,82281-26-3) + (3aR*,7R*,7aS*)-N-benzyl-2-oxo-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole (82281-26-3)

Guidance literature:

In xylene; at 150 ℃; for 3.5h; resealable glass bomb;

DOI:10.1021/jo00140a008

upstream raw materials:

(E)-N-benzyl-N-<<3,4-(methylnenedioxy)benzylidene>methyl>-3(E),5-hexadienamide

(E)-N-benzyl-N-<<3,4-(methylenedioxy)benzylidene>methyl>-2-(2,5-dihydro-1,1-dioxothienyl)acetamide

[2-Benzo[1,3]dioxol-5-yl-eth-(Z)-ylidene]-benzyl-amine

2-(2,5-Dihydro-1,1-dioxothienyl)acetyl chloride

Downstream raw materials:

(3aR*,7R*,7aR*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

(3aR*,7S*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

(3aR*,7R*,7aS*)-N-benzyl-7-<3,4-(methylenedioxy)phenyl>-2,3,3a,6,7,7a,-hexahydroindole

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