((triphenylphosphine)selenourea)gold(I) chloride*0.5(acetonitrile)

Base Information

Chemical Name:((triphenylphosphine)selenourea)gold(I) chloride*0.5(acetonitrile)
CAS No.:137039-52-2
Molecular Formula:0C₂H₃N*C₁₉H₁₉AuN₂PSe*Cl
Molecular Weight:638.253
Hs Code.:

Synonyms:((triphenylphosphine)selenourea)gold(I) chloride*0.5(acetonitrile)

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Chemical Property of ((triphenylphosphine)selenourea)gold(I) chloride*0.5(acetonitrile)

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Technology Process of ((triphenylphosphine)selenourea)gold(I) chloride*0.5(acetonitrile)

There total 1 articles about ((triphenylphosphine)selenourea)gold(I) chloride*0.5(acetonitrile) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 630-10-4
selenourea

: 137039-52-2
((triphenylphosphine)selenourea)gold(I) chloride*0.5(acetonitrile)

Guidance literature:: In acetone; (N2); soln. of Au-compound in acetone added to SeC(NH2)2 in acetone with stirring; stirred for 1 h; evapn. to dryness; recrystn. from CH3CN/CH3OH at 70°C; elem. anal.;

Reference yield: 86.0%

: 137039-52-2
((triphenylphosphine)selenourea)gold(I) chloride*0.5(acetonitrile)

: 137039-56-6
μ-selenido{bis(triphenylphosphine)gold(I)*dichloromethane

Guidance literature:: With Na₂CO₃; In methanol; water; (N2); addn. of Na2CO3 in H2O to soln. of Au-compound in CH3OH at -10°C with stirring; stirring for 1 h at -10°C; warming to room temp. within 3 h; stirring at 40°C for 1 h; addn. of CH2Cl2; org. layer is sepd.; aq. layer extd. with CH2Cl2; layers combined; dried with MgSO4; evapd. to dryness; recrystn. from CH2Cl2/CH3OH; elem. anal.;