Pseudo-geminal 2,11-Dithia<3.3>(2,5)pyrimidinophane

Base Information

• Chemical Name: Pseudo-geminal 2,11-Dithia<3.3>(2,5)pyrimidinophane
• CAS No.: 126504-94-7
• Molecular Formula: C₁₂H₁₂N₄S₂
• Molecular Weight: 276.386
• Mol file: 126504-94-7.mol

Synonyms:Pseudo-geminal 2,11-Dithia<3.3>(2,5)pyrimidinophane

Chemical Property of Pseudo-geminal 2,11-Dithia<3.3>(2,5)pyrimidinophane

Chemical Property:

Purity/Quality:

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Technology Process of Pseudo-geminal 2,11-Dithia<3.3>(2,5)pyrimidinophane

There total 1 articles about Pseudo-geminal 2,11-Dithia<3.3>(2,5)pyrimidinophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-dimethylpyrimidine (22868-76-4,144384-91-8) → Pseudo-geminal 2,11-Dithia<3.3>(2,5)pyrimidinophane (126504-94-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 38 percent / N-chlorosuccinimide (NCS), dibenzoyl peroxide / CCl₄ / 24 h / Heating; 2 equivalents NCS

2: 3 percent / cesium hydroxide monohydrate / methanol; dimethylformamide; H₂O / 2 h / Heating

With cesium hydroxide; N-chloro-succinimide; dibenzoyl peroxide; In methanol; tetrachloromethane; water; N,N-dimethyl-formamide;

upstream raw materials:

2,5-dimethylpyrimidine