9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde

Base Information

• Chemical Name: 9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde
• CAS No.: 1402660-09-6
• Molecular Formula: C₃₅H₃₁N₃O₅
• Molecular Weight: 573.648

Synonyms:9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde

Chemical Property of 9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde

Chemical Property:

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Technology Process of 9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde

There total 3 articles about 9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole (1252660-23-3) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde (1402660-09-6)

Guidance literature:

With trichlorophosphate; In 1,2-dichloro-ethane; at 0 - 90 ℃; for 48h;

DOI:10.1016/j.dyepig.2012.05.015

Reference yield:

2-(4-methoxyphenyl)-5-(4-hydroxyphenyl)-[1,3,4]oxadiazole (1252660-25-5) → 9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde (1402660-09-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 24 h / 100 °C / Inert atmosphere

2: trichlorophosphate / 1,2-dichloro-ethane / 48 h / 0 - 90 °C

With potassium carbonate; potassium iodide; trichlorophosphate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1016/j.dyepig.2012.05.015

Reference yield:

N-(6-bromohexyl)carbazole (94847-10-6) → 9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde (1402660-09-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 24 h / 100 °C / Inert atmosphere

2: trichlorophosphate / 1,2-dichloro-ethane / 48 h / 0 - 90 °C

With potassium carbonate; potassium iodide; trichlorophosphate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1016/j.dyepig.2012.05.015

upstream raw materials:

2-(4-methoxyphenyl)-5-(4-hydroxyphenyl)-[1,3,4]oxadiazole

9-(6-(4-(5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole

N,N-dimethyl-formamide

N-(6-bromohexyl)carbazole

Downstream raw materials:

C₅₉H₄₅N₉O₃

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