(S)-2-[3-(4-benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propylsulfanyl]-benzoic acid methyl ester

Base Information

• Chemical Name: (S)-2-[3-(4-benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propylsulfanyl]-benzoic acid methyl ester
• CAS No.: 932725-49-0
• Molecular Formula: C₂₉H₃₃NO₅S
• Molecular Weight: 507.651

Synonyms:(S)-2-[3-(4-benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propylsulfanyl]-benzoic acid methyl ester

Chemical Property of (S)-2-[3-(4-benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propylsulfanyl]-benzoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (S)-2-[3-(4-benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propylsulfanyl]-benzoic acid methyl ester

There total 1 articles about (S)-2-[3-(4-benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propylsulfanyl]-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

O-benzyl N-Boc-L-tyrosinol (66605-58-1) + Methyl thiosalicylate (4892-02-8) → (S)-2-[3-(4-benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propylsulfanyl]-benzoic acid methyl ester (932725-49-0)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.10.126

Reference yield:

(S)-2-[3-(4-benzyloxy-phenyl)-2-tert-butoxycarbonylamino-propylsulfanyl]-benzoic acid methyl ester (932725-49-0) → C24H25NO3S*ClH (932725-57-0)

Guidance literature:

With hydrogenchloride; water; In methanol; at 20 ℃; for 0.75h;

DOI:10.1016/j.bmcl.2009.10.126

upstream raw materials:

O-benzyl N-Boc-L-tyrosinol

Methyl thiosalicylate

Downstream raw materials:

C₂₄H₂₅NO₃S*ClH

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