RuP₁QH₂

Base Information

• Chemical Name: RuP₁QH₂
• CAS No.: 112220-06-1
• Molecular Formula: C₄₅H₃₈N₈O₄Ru*2F₆P
• Molecular Weight: 1145.85

Synonyms:RuP₁QH₂

Chemical Property of RuP₁QH₂

Chemical Property:

Purity/Quality:

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Technology Process of RuP₁QH₂

There total 1 articles about RuP₁QH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

ammonium hexafluorophosphate + RuP1DMB (112219-96-2) → RuP1QH2 (112220-06-1)

Guidance literature:

With BBr₃; In dichloromethane; mixture of RuP1DMB and BBr3 in CH2Cl2 stirred at -70 ° C for 4 h; soln. warmed to 0 ° C and treated with methanol; solvent evaporated and red solid dissolved in H2O and pptd. with NH4PF6; obtained complex dried under vacuum and purified chromatographically (on Al2O3 Using CH2Cl2/CH3CN, pure CH3CN and CH3OH/CH3CN as eluants); RuP1QH2 finally dissolved in CH3CN and pptd. from diethyl ether; elem. anal.;

DOI:10.1021/ja00212a029

Reference yield:

RuP1QH2 (112220-06-1) + 2,3-dicyano-5,6-dichloro-p-benzoquinone (84-58-2) → RuP1Q (112220-15-2)

Guidance literature:

In acetone; soln. of RuP1QH2 and DDQ in dry acetone allowed to stand in the dark for several hours under Ar; metal complex separated by dropping the reaction soln. into diethyl ether; solid RuP1Q filtered off and dried in vacuo;

DOI:10.1021/ja00212a029

upstream raw materials:

RuP₁DMB

Downstream raw materials:

RuP₁Q

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