5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-N⁴,2'-O-dimethylcytidine

Base Information

• Chemical Name: 5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-N⁴,2'-O-dimethylcytidine
• CAS No.: 1431457-37-2
• Molecular Formula: C₃₀H₄₅N₃O₈Si₃
• Molecular Weight: 659.959

Synonyms:5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-N⁴,2'-O-dimethylcytidine

Chemical Property of 5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-N⁴,2'-O-dimethylcytidine

Chemical Property:

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Technology Process of 5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-N⁴,2'-O-dimethylcytidine

There total 1 articles about 5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-N⁴,2'-O-dimethylcytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N4,2′-O-dimethylcytidine + benzhydryloxy-bis(trimethylsilyloxy)silyl chloride (309963-45-9) → 5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-N4,2'-O-dimethylcytidine (1431457-37-2)

Guidance literature:

N⁴,2′-O-dimethylcytidine; With diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;

benzhydryloxy-bis(trimethylsilyloxy)silyl chloride; In dichloromethane; N,N-dimethyl-formamide; for 0.166667h; Inert atmosphere;

DOI:10.1016/j.bmc.2013.03.010

Reference yield: 75.0%

5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-N4,2'-O-dimethylcytidine (1431457-37-2) + bis(N,N-diisopropylamino)methoxyphosphine (89437-96-7) → 5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-3'-O-(N,N-diisopropylamino)methoxyphosphonyl-N4,2'-O-dimethylcytidine (1431457-39-4)

Guidance literature:

With 1H-tetrazole; In dichloromethane; for 12h; Inert atmosphere;

DOI:10.1016/j.bmc.2013.03.010

upstream raw materials:

benzhydryloxy-bis(trimethylsilyloxy)silyl chloride

Downstream raw materials:

5'-O-benzhydryloxy-bis(trimethylsilyloxy)silyl-3'-O-(N,N-diisopropylamino)methoxyphosphonyl-N⁴,2'-O-dimethylcytidine

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