3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid

Base Information

Chemical Name:3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid
CAS No.:887914-42-3
Molecular Formula:C₄₇H₇₈O₉
Molecular Weight:787.131
Hs Code.:

Synonyms:3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid

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Chemical Property of 3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid

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Technology Process of 3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid

There total 8 articles about 3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 887914-41-2
3,5-bis(11-hydroxyundecyloxy)-4-dodecyloxybenzoic acid

: 814-68-6,25189-84-8
acryloyl chloride

: 887914-42-3
3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid

Guidance literature:: 3,5-bis(11-hydroxyundecyloxy)-4-dodecyloxybenzoic acid; acryloyl chloride; With N,N-diethylaniline; In 1,4-dioxane; at 60 ℃; for 3h;

With pyridine; water; at 80 ℃; for 1h;
DOI:10.1021/ja0606935

Reference yield:

: 887914-38-7
ethyl 3,5-bis[(tert-butyldimethylsilyl)oxy]-4-hydroxybenzoate

: 887914-42-3
3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: 94 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 10 h / 20 °C

2.1: 100 percent / tetrabutylammonium fluoride / CH₂Cl₂ / 10 h / 20 °C

3.1: K₂CO₃ / dimethylformamide / 6 h / 70 °C

4.1: 1.86 g / KOH / ethanol; H₂O / 3 h / Heating

5.1: N,N-diethylaniline / dioxane / 3 h / 60 °C

5.2: 71 percent / water; pyridine / 1 h / 80 °C

With potassium hydroxide; tetrabutyl ammonium fluoride; potassium carbonate; triphenylphosphine; N,N-diethylaniline; diethylazodicarboxylate; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 1.1: Mitsunobu reaction;
DOI:10.1021/ja0606935

Reference yield:

: 887914-40-1
ethyl 4-(dodecyloxy)-3,5-dihydroxybenzoate

: 887914-42-3
3,5-bis(11-acryloyloxyundecyloxy)-4-dodecyloxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / dimethylformamide / 6 h / 70 °C

2.1: 1.86 g / KOH / ethanol; H₂O / 3 h / Heating

3.1: N,N-diethylaniline / dioxane / 3 h / 60 °C

3.2: 71 percent / water; pyridine / 1 h / 80 °C

With potassium hydroxide; potassium carbonate; N,N-diethylaniline; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ja0606935