rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene)

Base Information

Chemical Name:rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene)
CAS No.:177161-77-2
Molecular Formula:C₄₁H₅₈O₃
Molecular Weight:598.91
Hs Code.:

Synonyms:rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene)

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Technology Process of rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene)

There total 3 articles about rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 19218-94-1
1-iodotetradecane

: 177161-76-1
rac-1-(pent-4-enyloxy)-3-(triphenylmethoxy)propan-2-ol

: 177161-77-2
rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene)

Guidance literature:: With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In diethyl ether; for 192h; Heating;
DOI:10.1002/hlca.19960790209

Reference yield:

: 177161-75-0
3-(pent-4-enyloxy)propane-1,2-diol

: 177161-77-2
rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene)

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / 24 h / Heating

2: 50 percent / 12N KOH, Bu₄N(HSO₄) / diethyl ether / 192 h / Heating

With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In pyridine; diethyl ether;
DOI:10.1002/hlca.19960790209

Reference yield:

: 177161-74-9
rac-5-<2,3-(isopropylidenedioxy)propyloxy>pent-1-ene

: 177161-77-2
rac-1,1',1-{[3-(pent-4-enyloxy)-2-(tetradecyloxy)propyloxy]methylidyne}tris(benzene)

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 2N HCl / methanol; H₂O / 4 h / Heating

2: 84 percent / pyridine / 24 h / Heating

3: 50 percent / 12N KOH, Bu₄N(HSO₄) / diethyl ether / 192 h / Heating

With hydrogenchloride; potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In pyridine; methanol; diethyl ether; water;
DOI:10.1002/hlca.19960790209