5-(3-chlorophenyl)-1,3,5,7,9,10-hexahydropyrimido[5',4'-5,6]pyridine[2,3-d]pyrimidine-2,4,6,8-tetraone

Base Information

Chemical Name:5-(3-chlorophenyl)-1,3,5,7,9,10-hexahydropyrimido[5',4'-5,6]pyridine[2,3-d]pyrimidine-2,4,6,8-tetraone
CAS No.:1374787-86-6
Molecular Formula:C₁₅H₁₀ClN₅O₄
Molecular Weight:359.728
Hs Code.:

Synonyms:5-(3-chlorophenyl)-1,3,5,7,9,10-hexahydropyrimido[5',4'-5,6]pyridine[2,3-d]pyrimidine-2,4,6,8-tetraone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(3-chlorophenyl)-1,3,5,7,9,10-hexahydropyrimido[5',4'-5,6]pyridine[2,3-d]pyrimidine-2,4,6,8-tetraone

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Technology Process of 5-(3-chlorophenyl)-1,3,5,7,9,10-hexahydropyrimido[5',4'-5,6]pyridine[2,3-d]pyrimidine-2,4,6,8-tetraone

There total 2 articles about 5-(3-chlorophenyl)-1,3,5,7,9,10-hexahydropyrimido[5',4'-5,6]pyridine[2,3-d]pyrimidine-2,4,6,8-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 67-52-7,944357-77-1
BARBITURIC ACID

: 587-04-2
m-Chlorobenzaldehyde

: 1374787-86-6
5-(3-chlorophenyl)-1,3,5,7,9,10-hexahydropyrimido[5',4'-5,6]pyridine[2,3-d]pyrimidine-2,4,6,8-tetraone

Guidance literature:: With ammonium acetate; N,N-diisopropylethylammonium acetate; at 20 ℃; for 0.75h;
DOI:10.1039/c8nj04622k

Reference yield: 85.0%

: 873-83-6
4-Amino-2,6-dihydroxypyrimidine

: 587-04-2
m-Chlorobenzaldehyde

: 1374787-86-6
5-(3-chlorophenyl)-1,3,5,7,9,10-hexahydropyrimido[5',4'-5,6]pyridine[2,3-d]pyrimidine-2,4,6,8-tetraone

Guidance literature:: With SBA-15 supported sulfonic acid nanocatalyst; In neat (no solvent); at 120 ℃; for 0.5h;
DOI:10.1007/s13738-015-0604-1