2-{1R,3S-3-[2-(3-Cyanophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic Acid

Base Information

• Chemical Name: 2-{1R,3S-3-[2-(3-Cyanophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic Acid
• CAS No.: 710281-43-9
• Molecular Formula: C₂₇H₂₈N₂O₅
• Molecular Weight: 460.53

Synonyms:2-{1R,3S-3-[2-(3-Cyanophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic Acid

Chemical Property of 2-{1R,3S-3-[2-(3-Cyanophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic Acid

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-{1R,3S-3-[2-(3-Cyanophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic Acid

There total 2 articles about 2-{1R,3S-3-[2-(3-Cyanophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

zinc(II) cyanide (557-21-1) + 2-{1R,3S-3-[2-(3-bromophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic acid (710281-44-0) → 2-{1R,3S-3-[2-(3-Cyanophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic Acid (710281-43-9)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In DMF (N,N-dimethyl-formamide); at 100 ℃; for 12h; Heating / reflux;

Reference yield:

2-{1R,3S-3-[2-(3-bromophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic acid (710281-44-0) + 2-(3-bromophenyl)-4-iodomethyl-5-methyloxazole (501362-90-9) + methyl 2-((1R,3S)-3-hydroxycyclohexyloxymethyl)-6-methylbenzoate (710281-31-5) + argon → 2-{1R,3S-3-[2-(3-Cyanophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic Acid (710281-43-9)

Guidance literature:

tetrakis(triphenylphosphine)palladium ⁽⁰⁾; In N-methyl-acetamide; water;

upstream raw materials:

2-{1R,3S-3-[2-(3-bromophenyl)-5-methyloxazol-4-ylmethoxy]cyclohexyloxymethyl}-6-methylbenzoic acid

2-(3-bromophenyl)-4-iodomethyl-5-methyloxazole

methyl 2-((1R,3S)-3-hydroxycyclohexyloxymethyl)-6-methylbenzoate

zinc(II) cyanide

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