C₅₃H₆₆O₂₄S

Base Information

Chemical Name:C₅₃H₆₆O₂₄S
CAS No.:870192-91-9
Molecular Formula:C₅₃H₆₆O₂₄S
Molecular Weight:1119.16
Hs Code.:

C<sub>53</sub>H<sub>66</sub>O<sub>24</sub>S

Synonyms:C₅₃H₆₆O₂₄S

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Chemical Property of C₅₃H₆₆O₂₄S

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Technology Process of C₅₃H₆₆O₂₄S

There total 21 articles about C₅₃H₆₆O₂₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 870192-88-4
C₇₂H₈₀O₂₄S

: 870192-91-9
C₅₃H₆₆O₂₄S

Guidance literature:: With acetic acid; at 60 ℃;
DOI:10.1016/j.bmcl.2005.08.019

Reference yield:

: 572-10-1,4451-35-8,4451-36-9,14227-52-2,14227-87-3,14227-88-4,14257-40-0,17081-03-7,19186-60-8,57237-01-1,65982-17-4,65982-18-5,65982-19-6,66966-08-3,144299-57-0
2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl chloride

: 870192-91-9
C₅₃H₆₆O₂₄S

Guidance literature:: Multi-step reaction with 13 steps

1: 50 °C

2: 89 percent / NaOMe / methanol / -25 °C

3: dimethylformamide

4: acetonitrile

5: NaOMe / methanol

6: CSA / dimethylformamide

7: 93 percent / pyridine

8: 94 percent / TBAF; 4 Angstroem molecular sieves / tetrahydrofuran

9: 86 percent / aq. AcOH / 65 °C

10: TEMPO; PhI(OAc)2 / CH₂Cl₂; H₂O

11: diethyl ether

12: 73 percent / TESOTf / CH₂Cl₂ / -78 °C

13: 80 percent / aq. AcOH / 60 °C

With pyridine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; 4 A molecular sieve; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; triethylsilyl trifluoromethyl sulfonate; sodium methylate; acetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 3: Michael addition;
DOI:10.1016/j.bmcl.2005.08.019

Reference yield:

: 870192-80-6
(2S,3S,4S,5R,6S)-4,5-Diacetoxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-carboxylic acid methyl ester

: 870192-91-9
C₅₃H₆₆O₂₄S

Guidance literature:: Multi-step reaction with 7 steps

1: 83 percent / pyridine / CH₂Cl₂

2: 81 percent / NaH

3: 86 percent / aq. AcOH / 65 °C

4: TEMPO; PhI(OAc)2 / CH₂Cl₂; H₂O

5: diethyl ether

6: 73 percent / TESOTf / CH₂Cl₂ / -78 °C

7: 80 percent / aq. AcOH / 60 °C

With pyridine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; triethylsilyl trifluoromethyl sulfonate; sodium hydride; acetic acid; In diethyl ether; dichloromethane; water;
DOI:10.1016/j.bmcl.2005.08.019