methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate

Base Information

Chemical Name:methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate
CAS No.:1410795-76-4
Molecular Formula:C₃₉H₅₂N₆O₂S₂
Molecular Weight:701.013
Hs Code.:

Synonyms:methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate

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Chemical Property of methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate

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Technology Process of methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate

There total 3 articles about methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 7753-72-2
methyl 3,7-dioxocholan-24-oate

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: 1410795-76-4
methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate

Guidance literature:: With hydrogenchloride; aluminum oxide; In neat (no solvent); for 0.0833333h; Microwave irradiation;
DOI:10.1016/j.bmcl.2012.09.083

Reference yield:

: 474-25-9
chenodeoxycholic acid

: 1410795-76-4
methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid

2: pyridinium chlorochromate / dichloromethane / 24 h / 20 °C

3: aluminum oxide; acetic acid / neat (no solvent) / 0.08 h / Microwave irradiation; Green chemistry

With aluminum oxide; toluene-4-sulfonic acid; acetic acid; pyridinium chlorochromate; In dichloromethane;
DOI:10.2174/157017812802850212

Reference yield:

: 28050-38-6
methyl 3β,7α-dihydroxy-5β-cholan-24-oate

: 1410795-76-4
methyl (5β)-3,7-bis[2-[(phenylamino)thioxomethyl]hydrazinylidene]-cholan-24-oate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium chlorochromate / dichloromethane

2: aluminum oxide; hydrogenchloride / neat (no solvent) / 0.08 h / Microwave irradiation

With hydrogenchloride; aluminum oxide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/j.bmcl.2012.09.083