1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile

Base Information

Chemical Name:1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile
CAS No.:775303-49-6
Molecular Formula:C₁₁H₁₈N₄O
Molecular Weight:222.29
Hs Code.:

Synonyms:1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile

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Chemical Property of 1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile

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Technology Process of 1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile

There total 1 articles about 1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 16603-49-9
1-(hydroxyamino)-3-methylcyclohexanecarbonitrile

: 54255-11-7
2-chloro-4,5-dihydro-1H-imidazole

: 775303-49-6
1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1002/ejoc.200400229

Reference yield: 39.0%

: 75-15-0,12122-00-8
carbon disulfide

: 775303-49-6
1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile

: 775303-52-1
3-methyl-1-({[(2-oxoimidazolidin-1-yl)carbonothioyl]thio}amino)cyclohexanecarbonitrile

Guidance literature:: With triethylamine; In acetone; at 20 ℃; for 20h;
DOI:10.1002/ejoc.200400229

Reference yield:

: 775303-49-6
1-[(4,5-dihydro-1H-imidazol-2-yloxy)amino]-3-methylcyclohexanecarbonitrile

: N-{2-[({[(1-cyano-3-methylcyclohexyl)amino]thio}carbonothioyl)amino]ethyl}pyrrolidine-1-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / Et₃N / acetone / 20 h / 20 °C

2: 55 percent / tetrahydrofuran / 20 h / 20 °C

With triethylamine; In tetrahydrofuran; acetone;
DOI:10.1002/ejoc.200400229