N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide

Base Information

Chemical Name:N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide
CAS No.:928783-05-5
Molecular Formula:C₂₄H₁₅Cl₄F₃N₄O₃
Molecular Weight:606.215
Hs Code.:

Synonyms:N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide

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Chemical Property of N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide

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Technology Process of N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide

There total 3 articles about N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 864736-87-8
1,2,3-trichloro-5-(1,1,1-trifluoroprop-2-en-2-yl)benzene

: 928783-10-2
N-acetyl-N-(5-chloro-2-pyrimidinyl)-4-hydroxyiminomethyl-2-methyl benzoic acid amide

: 928783-05-5
N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide

Guidance literature:: N-acetyl-N-(5-chloro-2-pyrimidinyl)-4-hydroxyiminomethyl-2-methyl benzoic acid amide; With N-chloro-succinimide; In 1,2-dimethoxyethane; at 40 ℃; for 0.5h;

1,2,3-trichloro-5-(1,1,1-trifluoroprop-2-en-2-yl)benzene; With water; potassium hydrogencarbonate; In 1,2-dimethoxyethane; at 20 ℃; for 1.5h;

Reference yield:

: 928783-08-8
N-(5-chloro-2-pyrimidyl)-4-formyl-2-methyl benzoic acid amide

: 928783-05-5
N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dmap / tert-butyl methyl ether / 4 h / 20 °C

2.1: hydroxylamine hydrochloride / methanol; water / 4 h / 20 °C

3.1: N-chloro-succinimide / 1,2-dimethoxyethane / 0.5 h / 40 °C

3.2: 1.5 h / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; triethylamine; dmap; In methanol; 1,2-dimethoxyethane; tert-butyl methyl ether; water;

Reference yield:

: 928783-09-9
N-acetyl-N-(5-chloro-2-pyrimidinyl)-4-formyl-2-methyl benzoic acid amide

: 928783-05-5
N-acetyl-N-(5-chloro-2-pyrimidinyl)-2-methyl-4-[5-(3,4,5-trichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole-3-yl] benzoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride / methanol; water / 4 h / 20 °C

2.1: N-chloro-succinimide / 1,2-dimethoxyethane / 0.5 h / 40 °C

2.2: 1.5 h / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; In methanol; 1,2-dimethoxyethane; water;