Technology Process of C25H26N2O2
There total 3 articles about C25H26N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 1.08 h / -78 °C
2.2: 12.5 h / -78 - 20 °C
3.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.17 h / 0 °C
3.2: 12.5 h / 0 - 20 °C
4.1: formic acid / 20 °C
With
formic acid; potassium tert-butylate; sodium hydride; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201200867
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1.08 h / -78 °C
1.2: 12.5 h / -78 - 20 °C
2.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.17 h / 0 °C
2.2: 12.5 h / 0 - 20 °C
3.1: formic acid / 20 °C
With
formic acid; potassium tert-butylate; lithium diisopropyl amide;
In
tetrahydrofuran; tert-butyl alcohol;
DOI:10.1002/chem.201200867
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.17 h / 0 °C
1.2: 12.5 h / 0 - 20 °C
2.1: formic acid / 20 °C
With
formic acid; potassium tert-butylate;
In
tetrahydrofuran; tert-butyl alcohol;
DOI:10.1002/chem.201200867