(2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene

Base Information

Chemical Name:(2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene
CAS No.:130487-35-3
Molecular Formula:C₂₆H₃₅NO₃
Molecular Weight:409.569
Hs Code.:

Synonyms:(2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene

Suppliers and Price of (2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene

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Technology Process of (2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene

There total 1 articles about (2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130487-34-2
(6E)-8-Benzyloxy-2-benzyloxymethyl-3-dimethylamino-6-methyl-1,6-octadiene

: 130487-35-3
(2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene

Guidance literature:: With peracetic acid; sodium carbonate; Yield given. Multistep reaction; 1) dichloromethane, -60 deg C, 30 min, 2) 40-50 deg C, 1 h;
DOI:10.1246/bcsj.63.1328

Reference yield: 100.0%

: 130487-35-3
(2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene

: 130487-36-4
(2Z,6E)-8-Benzyloxy-2-benzyloxymethyl-6-methyl-2,6-octadien-1-ol

Guidance literature:: With zinc; In water; acetic acid; for 24h; Ambient temperature;
DOI:10.1246/bcsj.63.1328

Reference yield:

: 130487-35-3
(2E,6E)-8-Benzyloxy-2-benzyloxymethyl-1-dimethylaminooxy-6-methyl-2,6-octadiene

: 130487-37-5
(2E,6E)-1,8-Bis(benzyloxy)-2-chloromethyl-6-methyl-2,6-octadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / zinc dust / acetic acid; H₂O / 24 h / Ambient temperature

2: lithium chloride, γ-collidine, methanesulfonyl chloride / dimethylformamide / 2 h / 0 °C

With 2,4,6-trimethyl-pyridine; methanesulfonyl chloride; lithium chloride; zinc; In water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.63.1328