benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

Base Information

Chemical Name:benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside
CAS No.:89342-59-6
Molecular Formula:C₃₇H₄₆O₁₀
Molecular Weight:650.766
Hs Code.:

Synonyms:benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

Suppliers and Price of benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

There total 10 articles about benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.5%

: 89315-94-6
benzyl O-(2,4-di-O-benzyl-3-O-methyl-6-O-trityl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

: 89315-95-7
benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-α-L-rhamnopyranoside

: 89342-59-6
benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

Guidance literature:: With acetic acid; In methanol; water; for 1h; Heating;
DOI:10.1016/S0008-6215(00)90396-3

Reference yield: 4.3%

: 104731-80-8
benzyl O-(2,3,4-tri-O-benzyl-6-O-trityl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

: 89342-59-6
benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

: 104731-81-9
benzyl O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1<*>4)-α-L-rhamnopyranoside

Guidance literature:: With acetic acid; In methanol; water; for 1.5h; Heating;
DOI:10.1016/S0008-6215(00)90396-3

Reference yield:

: 53270-14-7
benzyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

: 89342-59-6
benzyl O-(2,4-di-O-benzyl-3-O-methyl-β-D-glucopyranosyl)-(1<*>4)-2,3-O-isopropylidene-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 86.1 percent / mercury cyanide / acetonitrile / 5 h / Ambient temperature

2: 1.) sodium methoxide, 2.) pyridine / 1.) MeOH, 2.) 80 deg C, 3 h, RT, 2 d, 3.) RT

3: 83.2 percent / potassium hydroxide / 2 h / 130 - 140 °C

4: 4.3 percent / 60percent acetic acid / methanol / 1 h / Heating

With pyridine; potassium hydroxide; sodium methylate; mercury(II) cyanide; acetic acid; In methanol; acetonitrile;
DOI:10.1016/S0008-6215(00)90396-3