benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxy-2',3'-O-isopropylidene-adenosine]-propylcarbamate

Base Information

• Chemical Name: benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxy-2',3'-O-isopropylidene-adenosine]-propylcarbamate
• CAS No.: 548483-91-6
• Molecular Formula: C₂₄H₂₉N₇O₉S
• Molecular Weight: 591.602

Synonyms:benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxy-2',3'-O-isopropylidene-adenosine]-propylcarbamate

Chemical Property of benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxy-2',3'-O-isopropylidene-adenosine]-propylcarbamate

Chemical Property:

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Technology Process of benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxy-2',3'-O-isopropylidene-adenosine]-propylcarbamate

There total 1 articles about benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxy-2',3'-O-isopropylidene-adenosine]-propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

3-(benzyloxycarbonylamino)propanoic acid (2304-94-1) + ((3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl sulfamate (112921-00-3) → benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxy-2',3'-O-isopropylidene-adenosine]-propylcarbamate (548483-91-6)

Guidance literature:

With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 0 - 20 ℃;

DOI:10.1021/ol034212n

Reference yield: 80.0%

benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxy-2',3'-O-isopropylidene-adenosine]-propylcarbamate (548483-91-6) → benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxyadenosine]-propylcarbamate (548483-94-9)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 3h;

DOI:10.1021/ol034212n

upstream raw materials:

3-(benzyloxycarbonylamino)propanoic acid

((3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl sulfamate

Downstream raw materials:

benzyl 3-oxo-3-[5'-aminosulfamoyl-5'-deoxyadenosine]-propylcarbamate

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