benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside

Base Information

Chemical Name:benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside
CAS No.:693219-36-2
Molecular Formula:C₂₄H₃₈O₇Si
Molecular Weight:466.647
Hs Code.:

Synonyms:benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside

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Technology Process of benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside

There total 4 articles about benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 108-24-7
acetic anhydride

: 693219-35-1
benzyl 6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside

: 693219-36-2
benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2004.02.054

Reference yield:

: 4304-12-5,14897-46-2,15548-45-5,25320-99-4,34246-23-6,47000-20-4,53448-50-3,86196-36-3,133908-86-8
benzyl β-D-galactopyranoside

: 693219-36-2
benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 48 h / 20 °C

2: 93 percent / p-toluenesulfonic acid monohydrate / 3 h / 20 °C

3: 74 percent / triethylamine / CH₂Cl₂ / 48 h / 20 °C

With toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane;
DOI:10.1016/j.tet.2004.02.054

Reference yield:

: 693219-34-0
benzyl 6-O-(tert-butyldimethylsilyl)-β-D-galactopyranoside

: 693219-36-2
benzyl 2-O-acetyl-6-O-(tert-butyldimethylsilyl)-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / p-toluenesulfonic acid monohydrate / 3 h / 20 °C

2: 74 percent / triethylamine / CH₂Cl₂ / 48 h / 20 °C

With toluene-4-sulfonic acid; triethylamine; In dichloromethane;
DOI:10.1016/j.tet.2004.02.054