1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarboxylic acid bis-benzylamide

Base Information

Chemical Name:1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarboxylic acid bis-benzylamide
CAS No.:98608-91-4
Molecular Formula:C₂₈H₄₀N₄O₆
Molecular Weight:528.649
Hs Code.:

Synonyms:1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarboxylic acid bis-benzylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarboxylic acid bis-benzylamide

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Technology Process of 1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarboxylic acid bis-benzylamide

There total 2 articles about 1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarboxylic acid bis-benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 98608-86-7
1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarbonyl dichloride

: 100-46-9
benzylamine

: 98608-91-4
1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarboxylic acid bis-benzylamide

Guidance literature:: With triethylamine; In chloroform; at 20 ℃;
DOI:10.1007/BF00519159

Reference yield:

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 98608-91-4
1,4,10,13-Tetraoxa-7,16-diaza-cyclooctadecane-7,16-dicarboxylic acid bis-benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / pyridine / toluene / 0 °C

2: CHCl₃ / 0 - 5 °C

With pyridine; In chloroform; toluene;
DOI:10.1007/BF00519159