4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride

Base Information

Chemical Name:4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride
CAS No.:856452-72-7
Molecular Formula:C₁₆H₈Cl₃N₃O₃S
Molecular Weight:428.683
Hs Code.:

Synonyms:4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride

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Chemical Property of 4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride

Chemical Property:

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Technology Process of 4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride

There total 1 articles about 4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 853565-51-2
2-(5-Amino-[1,3,4]thiadiazol-2-yl)-4,6-dichloro-phenol

: 100-20-9
terephthaloyl chloride

: 856452-72-7
4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride

Guidance literature:: In tetrahydrofuran; acetone; at 20 ℃; for 0.5h;

Reference yield:

: 582-33-2
3-aminobenzoic acid ethyl ester

: 856452-72-7
4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride

: 3-{4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoylamino}-benzoic acid ethyl ester

Guidance literature:: 3-aminobenzoic acid ethyl ester; 4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride; With pyridine; In tetrahydrofuran; N,N-dimethyl-formamide; at 55 ℃; for 20h;

With hydrogenchloride; In water; isopropyl alcohol; at 20 ℃;

Reference yield:

: 856452-76-1
3-methyl-4-(1H-1,2,4-triazol-1-yl)aniline

: 856452-72-7
4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride

: N-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-yl]-N'-(3-methyl-4-[1,2,4]triazol-1-yl-phenyl)-terephthalamide

Guidance literature:: 3-methyl-4-(1H-1,2,4-triazol-1-yl)aniline; 4-[5-(3,5-Dichloro-2-hydroxy-phenyl)-[1,3,4]thiadiazol-2-ylcarbamoyl]-benzoyl chloride; With pyridine; In tetrahydrofuran; N,N-dimethyl-formamide; at 55 ℃; for 20h;

With hydrogenchloride; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); water; isopropyl alcohol; at 20 ℃;