Technology Process of C27H35N3O6
There total 19 articles about C27H35N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium nitrososulfonate;
In
ethyl acetate;
at 20 ℃;
for 0.5h;
aq. phosphate buffer;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium hydroxide / methanol; 1,2-dimethoxyethane; water / 1 h / 80 °C
2.1: trichlorophosphate / N,N-dimethyl-formamide / 1.5 h / 0 - 40 °C
2.2: 0.33 h / 0 °C / Reflux
3.1: ammonium acetate / 1.5 h / Reflux
4.1: borane-THF / tetrahydrofuran / 1.5 h / 70 °C
5.1: dmap; triethylamine / tetrahydrofuran / 16 h / 20 °C
6.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -10 °C
6.2: 0.25 h / 20 °C
6.3: 70 °C
7.1: palladium 10% on activated carbon; ammonium acetate / ethanol / 0.5 h / 45 °C
7.2: 12 h
8.1: potassium nitrososulfonate / ethyl acetate / 0.5 h / 20 °C / aq. phosphate buffer
With
dmap; n-butyllithium; borane-THF; potassium nitrososulfonate; palladium 10% on activated carbon; ammonium acetate; triethylamine; potassium hydroxide; trichlorophosphate;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; hexane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: borane-THF / tetrahydrofuran / 1.5 h / 70 °C
2.1: dmap; triethylamine / tetrahydrofuran / 16 h / 20 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -10 °C
3.2: 0.25 h / 20 °C
3.3: 70 °C
4.1: palladium 10% on activated carbon; ammonium acetate / ethanol / 0.5 h / 45 °C
4.2: 12 h
5.1: potassium nitrososulfonate / ethyl acetate / 0.5 h / 20 °C / aq. phosphate buffer
With
dmap; n-butyllithium; borane-THF; potassium nitrososulfonate; palladium 10% on activated carbon; ammonium acetate; triethylamine;
In
tetrahydrofuran; ethanol; hexane; ethyl acetate;
DOI:10.1002/chem.201103605
